MODULES ANALYSETTE 22
Measuring Unit / Laser Particle Sizer
ANALYSETTE 22
NanoTecEach measuring unit ANALYSETTE 22 NanoTec with USB-Interface, is delivered with a computer* with already installed software MaS control, monitor, keyboard and mouse.
*Except deliveries to CIS countries
Choose the perfect dispersion unit according to your measurement tasks!
Wet dispersion is the ideal dispersion method for most samples. For easily soluble samples or samples that swell significantly, dry dispersion or the falling chute is the right solution.
For representative sample division - the foundation of any precise analysis - we recommend the
Rotary Cone Sample Divider LABORETTE 27
Dispersion units
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Wet Dispersion Units - the ideal standard-solution for most samples
Dispersion module Measuring range Recommended dispersion liquid Suspension volume Wet dispersion unit
for wet measurement of solids and suspensions0.01 - 2100 µm water 300 – 500 ml AutoSampler for wet dispersion unit
for the automation of measurement series0.01 - 2100 µm water up to 26 containers at 40 ml Small volume wet dispersion unit SVA
for wet measurement of samples which are only available in a minimal quantity or in organic solvents with fully automatic dispersion0.01 - 600 µm almost all dispersion liquids 50 ml Small volume wet dispersion unit SVM
for wet measurement of small sample quantities with mechanical dispersion and intuitive manual operation0.01 - 600 µm water, organic solvents 100 ml -
Dry Dispersion Units - for slightly soluble or highly swellable samples
Dispersion module Measuring range Dispersion Sample volume Dry dispersion unit
for dry measurement of not too fine, free-flowing materials0.01 - 2100 µm Degradation of agglomerates with compressed air 1 – 100 cm3 Falling chute
for dry measurement of agglomerates of dry powders and easily free-flowing, coarse-grained materials without dispersion0.01 - 2100 µm Without dispersion and compressed air, agglomerates are preserved 1 – 100 cm3
Choose the perfect dispersion unit according to your measurement tasks!
- Wet Dispersion Units - the ideal standard-solution for most samples
- Dry Dispersion Units - for slightly soluble or highly swellable samples
Wet Dispersion Units
automatic dispersion unit, volume 300-500 ml, 100 Watt ultrasonic power
for 100-120/200-240 V/1~, 50-60 Hz, 100 Watt - voltage indicated by customer is set.
For most samples wet dispersion represents the ideal method for perfect dispersion. Therefore, the sample material is fed into a closed liquid circulation system. An integrated and freely programmable ultrasonic emitter with up to 100 Watt of ultrasonic power and adjustable dispersion conditions ensures fast and extremely efficient degradation of the agglomerates – precisely adapted to each sample.
Additional facts about the wet dispersion unit:
- Strong ultrasonic power of up to 100 Watt, freely adjustable
- Freely programmable
- Automatic rinsing cycle
- Variable suspension volume between 300 and 500 ml
- Extremely quiet dispersion
- Fast and consistent cleaning
- Benzine, alcohol and many organic solvents can also be used as suspension liquid as a standard feature
- No dead space in measuring and rinsing circulation system
Detailed information about the Wet Dispersion Unit
automatic dispersion unit, volume 50 ml, 100 Watt ultrasonic power
for 100-120/200-240 V/1~, 50/60 Hz, 120 Watt - voltage indicated by customer is set.
The small volume wet dispersion unit SVA ensures perfect, fully automatic dispersion of samples which are only available in a minimal quantity. For measurements in organic solvents, the unit needs less than 50 ml liquid. This minimises the disposal costs and decreases environmental pollution. It is ideal for measurements in solvents up to a particle size of about 600 μm.
Additional facts about the small volume wet dispersion unit SVA:
- Very small sample quantities in below 50 ml of liquid
- Almost all dispersion liquids can be used
- Resistant to chemicals
- Very strong and controllable ultrasonic power of 100 Watt
- Practical illuminated dispersion bath
- Automatic rinsing for fast cleaning
- No dead space in the liquid circulation system
- All functions are SOP-controlled
Detailed information about the Small Volume Wet Dispersion Unit SVA
Conversion kit Extended for extreme chemical resistance for small volume wet dispersion unit SVA - 22.8800.00.
Consists of seals, O-rings and flow plate made of FFKM Kalrez® – the hoses are made of Santoprene®.
If you are working with extremely aggressive chemical dispersion liquids, like for example acetone or dimethylketone, you can order the SVA dispersion unit with this conversion kit for extreme chemical resistance.
If you already have a unit, you can order the conversion kit separately and your equipment can be retrofitted.
You can download a list of chemicals for the different dispersion units here:
List of suitable chemicals
manual dispersion unit, volume 100 ml
for 230 V/1~, 50-60 Hz, 35 Watt
(Transformer to adapt line voltage on request!)
The small volume wet dispersion unit SVM is ideal for mechanical dispersion of very small sample quantities and offers intuitive manual operation. The unit needs 100 ml liquid for the entire measurement circuit, which is extremely important for the use of organic solvents. It is ideal for wet measurements up to a particle size of about 600 μm.
Additional facts about the small volume wet dispersion unit SVM:
- Practical transparent glass container for checking the sample
- Thorough rinsing of the measurement circuit, which has no dead space, with a single-lever valve (4/2- way ball valve)
- Manually controlled centrifugal pump for gentle transport of the sample
- Benzine, alcohol and many organic solvents can also be used as suspension liquid
Detailed information about the Small Volume Wet Dispersion Unit SVM
Dry Dispersion Units
for dispersion in a free jet with pre-dispersion
for 100-120/200-240 V/1~, 50-60 Hz, 50 Watt
Dry dispersion is especially suited for not too fine, free-flowing materials, which react in water or other liquids. The sample material is transported with a vibratory feeder through the intake funnel into the dry measuring cell, where it falls directly into a Venturi nozzle operating with an adjustable flow of compressed air. Upon passing through the nozzle, agglomerates are broken up and the measurement of the particle size distribution in the laser beam takes place directly behind it.
Additional facts about the dry dispersion unit:
- Fast measurement of powdery samples in an accelerated air flow
- For sample volumes from less than 1 cm3 to approx. 100 cm3
- Efficient degradation of agglomerates with a special annular gap Venturi nozzle
- No impact areas – protection against comminution of the particles
- Perfect sample feeding with high frequency feeder
- Automatic computer-controlled adjustment of the dispersion pressure
- Fully automatic, freely programmable measurement processes
- Especially fast and easy to clean
- Multifunctional exhaust system
- Conversion kit to use the dry dispersion unit as a falling chute
Detailed information about the dry Dispersion Unit
for feeding free-flowing samples
for 100-120/200-240 V/1~, 50-60 Hz, 50 Watt
For dry measurement of agglomerates of dry powder or for determining particle size distributions of free-flowing, coarse-grained materials without dispersion.
In this case, the sample is transported with an electronically controlled feeder directly above the intake funnel of the falling chute, from where it falls directly into the measuring cell and is measured by the laser beam without any dispersion at all.
Detailed information about the Falling Chute
For dry measurement without Dispersion.
For 100-120/200-240 V/1~, 50-60 Hz.
Cartridge with cpl. dry measuring cell incl. insertion block - for the use as a conversion kit - for insertion in the dry dispersion unit (article no. 22.8600.00).
For dry measurement of agglomerates of dry powder or for determining particle size distributions of free-flowing, coarse-grained materials without dispersion.
In this case, the sample is transported with an electronically controlled feeder directly above the intake funnel of the falling chute, from where it falls directly into the measuring cell and is measured by the laser beam without any dispersion at all.
Detailed information about the Falling Chute
AutoSampler for wet dispersion unit - 22.8500.00 for the automation of measurement series
For the automation of measurement series, incl. 40 ml Containers.
For 100-240 V/1~, 50-60 Hz, 30 Watt.
Ideal for efficient automation of measurement series: The practical FRITSCH AutoSampler provides automatic sample feeding as a simple attachment for the wet dispersion unit of the ANALYSETTE 22.
Additional facts about the AutoSampler:
- Work completely independently right from the start
- 26 positions for 40 ml standard containers
- Reliable complete sample feeding due to tilt function and programmable rinsing function with a strong water jet
- Automatic assignment of the position and measuring result via software
- All function sequences, such as the dispersion and measurement duration, can be specified for each position separately and can be saved as a SOP standard list
- Practical Home button for automatically returning to position 1
Detailed information about the AutoSampler
Detailed information about the Wet Dispersion Unit
Sample containers 40 ml with screw lid for the AutoSampler.
Reference materials and certificates
Reference materials for regular inspection of the Laser Particle Sizer ANALYSETTE 22 NanoTec to ensure proper function. The reference materials offered by FRITSCH are delivered along with precise dispersion and measurement instructions and are accompanied by a certificate that states the upper and lower limits of the expected particle sizes. These limit values were determined using an internationally recognised process (NIST-traceable).
Certified reference materials (NIST-traceable) for performance verification according to ISO 13320
Test powder for wet dispersion, 10 - 100 µm (Box with 10 single-shots 0.5 g), certified reference material for performance verification of the FRITSCH Laser Particle Sizer ANALYSETTE 22 NanoTec, which is used for wet dispersion and for calibration according to ISO 13320 in regard to repeatability and reproducibility.
The test powder for wet dispersion is delivered in a box with 10 single-shots 0.5 g.
Also test suspensions for the inspection of the measurement precision as well as a test powder for dry dispersion are offered.
Test powder for dry dispersion, 50 - 350 µm (box with 10 single-shots 5 g) certified reference material for performance verification of the FRITSCH Laser Particle Sizer ANALYSETTE 22 NanoTec, which is used for dry dispersion and for calibration according to ISO 13320 in regard to repeatability and reproducibility.
The test powder for dry dispersion is delivered in a box with 10 single-shots 5 g.
Also a test powder for wet dispersion, as well as test suspensions for the inspection of the measurement precision are offered.
Test suspension nano (approx. 200 nm) for system check (box with 10 single-shots 5 ml) for the inspection of the measurement precision of the FRITSCH Laser Particle Sizer ANALYSETTE 22 NanoTec, which is used for wet dispersion.
The test suspension nano for system check for wet dispersion is delivered in a box with 10 single-shots 5 ml.
Additional test suspensions for inspection of the measurement precision, as well as test powders for the calibration of the Laser Particle Sizer ANALYSETTE 22 NanoTec according to ISO 13320 in regard to repeatability and reproducibility are also offered.
Test suspension 1 µm for system check (Box with 10 single-shots 5 ml) for inspection of the measurement precision of the FRITSCH Laser Particle Sizer ANALYSETTE 22 NanoTec, which is used for wet dispersion.
The test suspension 1 µm for system check for wet dispersion is delivered in a box with 10 single-shots 5 ml.
Additional test suspensions for inspection of the measurement precision as well as test powders for the calibration of the Laser Particle Sizer ANALYETTE 22 NanoTec according to ISO 13320 in regard to repeatability and reproducibility are also offered.
Test suspension 10 µm for system check (Box with 10 single-shots 5 ml) for inspection of the measurement precision of the FRITSCH Laser Particle Sizer ANALYSETTE 22 NanoTec, which is used for wet dispersion.
The test suspension 10 µm for system check for wet dispersion is delivered in a box with 10 single-shots 5 ml.
Additional test suspensions for inspection of the measurement precision, as well as test powders for the calibration of the Laser Particle Sizer ANALYSETTE 22 NanoTec according to ISO 13320 in regard to repeatability and reproducibility are also offered.
FRITSCH reference materials according to ISO 13320
For calibration of the Laser Particle Sizer ANALYSETTE 22 NanoTec for wet and dry dispersion within the framework of a test equipment monitoring system as per ISO 13320.
The cost-efficient alternative (non-certified reference materials) for regular inspection of your Laser Particle Sizer ANALYSETTE 22.
The FRITSCH-test powder F-500, 0.5 - 50 µm is delivered in a handy 50 g bottle.
For calibration of the Laser Particle Sizer ANALYSETTE 22 NanoTec for dry dispersion within the framework of a test equipment monitoring system as per ISO 13320.
The cost-efficient alternative (non-certified reference materials) for regular inspection of your Laser Particle Sizer ANALYSETTE 22.
The FRITSCH-test powder F-70, 100 - 600 µm is delivered in a handy 150 g bottle.
Certification
Set of IQ/OQ blank forms, (questionnaire format – standards and implementation not included).
For the support of the initial operation resp. examination of the function of the FRITSCH Laser Particle Sizer according to ISO 13320, FRITSCH offers appropriate questionnaires as blank forms. Certificates for tests according to ISO 13320 available on request:
Certificates for tests according to ISO 13320 for ANALYSETTE 22 NanoTec
We offer the Performance Verification for the wet and dry dispersion. The verification must be carried out directly on the instrument either here in Idar-Oberstein or at your site. Therefore, we would like to provide you with an individual offer – according to your needs.
Performance Verification for wet dispersion – Order No. 96.0080.00
Performance Verification for dry dispersion – Order No. 96.0081.00
Just contact:
Mr. Stefan Fröhlich,
phone: 0049 67 84 70 150
froehlich@fritsch.de
